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石油学报（石油加工）ACTA PETROLEI SINICA(PETROLEUM PROCESSING SECTION)2004 V20 N1 P12-21--------------------------------------------------------------------------------EFFECT OF STEAM TREATMENT AND PHOSPHOROUS ACID MODIFICATION OF HZSM-5 ON ITS PHYSICOCHEMICAL AND CATALYTIC PROPERTIESAbstract：Physicochemical and catalytic properties of phosphorous acid modified HZSM�5 ze olites treated with 100% steam at 673，873，and 1073*!K have been T he structure of the samples was characterized by XRDThe acidity and distributio n of the acidic sites were studied by IR using pyridine as probe molecule and te mperature programmed desorption (TPD) of The state of phosph orus were studied by XPS，showing that P (Ⅲ) was oxidized to P (Ⅴ)，a model for the surface structure of the modification is Th e textural properties of catalysts determined by nitrogen isothermal adsorption �desorption measurements suggest the isothermal type of all samples is a combin ation of type Ⅰ and type Ⅳ，all hysteresis loops resemble the H4�type in the IUPAC The state of aluminum was characterized by 27 Al MAS N MR AM1 (Austin model) semi�empirical method and cluster model method have been employed to study the stability of two possible phosphor us modified zeolite geometries，the difference was the bridging oxygen of phosph orus coordination with aluminum or the terminal oxygen of phosphorus coordinatio n with The result showed that the terminal oxygen coordination was more possible according to the heat of formation (HF)The �n��heptane cracking reaction was selected as probe reaction to investigate the activity of studied �Keywords：HZSM�5 zeolites；steam treatment；phosphorous acid modificati on；texture；cracking activity 亚磷酸和水蒸气联合改性的HZSM-5的物化性质和催化性能研究吕仁庆 唐博 王震宇 王秋英 项寿鹤 摘 要：考察了由亚磷酸改性的HZSM-5在673、873和1073K温度下100%水蒸气处理样品的物化和催化性质采用XRD表征了样品的结构通过吸附吡啶红外光谱和NH3-TPD进行了酸性和酸分布研究XPS的研究结果表明,P由+3价氧化成了+5价,并提出了可能的改性的表面结构模型通过N2吸附-脱附等温线研究了样品的孔结构,样品的吸附-脱附等温线为Ⅰ型和Ⅳ型的复合型,滞后环为IUPAC分类的H4型Al的状态由27Al MAS NMS表征采用AM1(Austin Model Ⅰ)半经验量子化学方法和模型簇法筛选了磷改性可能的两种结构模型,其区别在于磷上的桥氧与铝配位还是端氧与铝配位,结果表明端氧与铝配位的可能性更大以正庚烷裂化反应为探针反应考察了样品的活性关键词：HZSM-5沸石;水热处理;亚磷酸改性;结构;裂化活性CLC Number：TE4 Document ID：AArticle ID：1001-8719(2004)01-0012-10 Foundation Item：国家自然科学基金(20233030)和石油大学中国石油天然气集团公司催化重点实验室资助项目Author Resume：吕仁庆(1969-),男,讲师,博士研究生,从事沸石催化研究;唐博(1964-),男,高级工程师,博士研究生,从事工业催化研究;王震宇(1974-),男,工程师,硕士,从事催化剂生产工作;王秋英(1964-),女,高级工程师,硕士,从事沸石催化研究:项寿鹤(1939-),男,教授,从事沸石合成与催化研究 通讯联系人:吕仁庆 Author Unit：吕仁庆（南开大学,化学系,天津,300071） 唐博（南开大学,化学系,天津,300071） 王震宇（南开大学,催化剂厂,天津,300071） 王秋英（南开大学,催化剂厂,天津,300071） 项寿鹤（南开大学,化学系,天津,300071） References：〔1〕Scherzer JOctane-enhancing,zeolitic FCC catalysts,scientific and technical aspects[J]Catal Rev-Sci Eng,1989,31(3):215-〔2〕Lischke G,Eckelt R,Jerschkewitz H-G,et Spectroscopic and physicochemical characterization of P-modified H-ZSM-5[J]J Catal,1991,132(1):229-〔3〕Kaeding W W,Chu C,Young L B,et Shape selective reactions with zeolite catalysts[J]J Catal,1981,69:392-〔4〕Jentys A,Rumplmayr G,Lerche r J AHydroxyl groups in 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HZSM-5 zeolite catalysts[J]J Catal,1990,124:224-〔20〕Suzuki K,Kiyozumi Y,Matsuzaki KEffect of modification of ZSM-5 type zeolite with calcium phosphate on its physico-chemical and catalytic properties[J]Appl Catal,1988,39:315-〔21〕Ikai S,Okamoto M,Nishioka H,et HZSM-5 pelletized and modified with α-Ca3(PO4)2 and HPO�42- as a catalyst for methanol conversion[J]Appl Catal,1989,49:143,〔22〕Shen Y F,Ko A N,Grange PStudy of phosphorus-modified aluminum pillared montmorillonite I Effect of the nature of phosphorus compounds[J]Appl Catal,1990,67:93-〔23〕Wu E L,Lawton S L,Olson D H,et ZSM-5-type material,factors affecting crystal symmetry[J]J Phys Chem,1979,83(21):2777-〔24〕Mastikhin V M,Zamaraev K IStudies of heterogeneous catalysis using high-resolution solid state NMR[J]Applied Magnetic Resonance,1990,1:295-〔25〕Lü R Q,Wang Q Y,Tang B,et Physicochemical characterization and catalytic study of steam combined with phosphorus modified HZSM-5[C]ZMPC2003 Symposium,August 3-6 in Sapporo,Japan,〔26〕Lischke G,Eckelt R,Jerschkewitz H-G,et Spectroscopic and physicochemical characterization of P-modified H-ZSM-5[J]J Catal,1991,132(1):229-〔27〕Wagner C D,Riggs W M,Davis L E,et Handbook of X-ray photoelectron spectroscopy,A reference book of standard data for use in X-ray photoelectron spectroscopy[M]Published by Perkin-Elmer Corporatio n physical electronics Division 6509 Flying Cloud drive Eden Prairie,Minnesota 〔28〕Dewar M J S,Zoebisch E G,Healy E F SAM1: A new general purpose quantum mechanical molecular model[J]J Am Chem Soc,1985,107:3902-Manuscript Received：2003年1月13日Published：2004年2月25日

中国石油大学华东，邮编:266555地址:青岛市黄岛区长江西路66号。可上学校官网查看，有详细介绍。

这是国内中文核心一些石油相关期刊，供您参考一下: 石油勘探与开发 石油学报 天然气工业 石油与天然气地质 石油化工 石油实验地质 石油大学学报自然科学版(中国石油大学学报自然科学版) 石油钻采工艺 油田化学 新疆石油地质 西南石油学院学报(改名为:西南石油大学学报) 石油机械 钻采工艺 石油炼制与化工 大庆石油地质与开发西安石油大学学报自然科学版 石油地球物理勘探 油气地质与采收率 油气储运 石油天然气学报中国海上油气 石油钻探技术 大庆石油学院学报 石油物探 油气田地面工程天然气地球科学 石油学报石油加工测井技术断块油气田 其中石油学报是EI部分收录。 国外SCI收录期刊主要有： AAPG BULLETIN 《美国石油地质学家协会通报》美国 BULLETIN OF CANADIAN PETROLEUM GEOLOGY 《加拿大石油地质学通报》加拿大 CHEMISTRY AND TECHNOLOGY OF FUELS AND OILS 《燃料与石油化学和工艺学》美国 China Petroleum Processing & Petrochemical Technology 《中国炼油与石油化工》中国 GEOARABIA 《中东石油地球科学杂志》巴林 HYDROCARBON PROCESSING 《烃加工》美国 INTERNATIONAL GAS Engineering AND MANAGEMENT 《国际天然气工程与管理》英国 JOURNAL OF CANADIAN PETROLEUM TECHNOLOGY 《加拿大石油技术杂志》加拿大 JOURNAL OF GEOPHYSICS AND ENGINEERING 《地球物理学与工程学》英国 JOURNAL OF PETROLEUM GEOLOGY 《石油地质学杂志》英国 JOURNAL OF Petroleum Science AND ENGINEERING《石油科学和石油工程杂志》荷兰 JOURNAL OF THE JAPAN PETROLEUM INSTITUTE 《日本石油学会志》日本 OIL & GAS JOURNAL 《石油与天然气杂志》美国 OIL & GAS SCIENCE AND TECHNOLOGY REVUE DE L INSTITUT FRANCAIS DU PETROLE 《石油、天然气的科学与技术；法国石油研究所杂志》法国 OIL GAS-EUROPEAN MAGAZINE 《欧洲石油气杂志》德国 OIL SHALE 《油页岩》爱沙尼亚 PETROLEUM CHEMISTRY 《石油化学》美国 PETROLEUM GEOSCIENCE 《石油地质科学》英国 PETROLEUM SCIENCE 《石油科学》德国 PETROLEUM SCIENCE AND TECHNOLOGY 《石油科学与技术》美国 PETROPHYSICS 《岩石物理学》美国 SPE DRILLING & COMPLETION 《石油工程师协会钻井与完井》美国 SPE JOURNAL 《石油工程师协会杂志》美国 SPE PRODUCTION & OPERATIONS 《石油工程师协会生产和操作》美国 SPE RESERVOIR EVALUATION & ENGINEERING 《石油工程师协会油藏评估与工程》美国 VISION TECNOLOGICA 《技术视野》委内瑞拉 SPE相对容易一些

这东西很多,但是还需要自己美化下,不然没有任何意义 参考资料：电脑软硬件应用网

主要刊登石油和天然气地质、地质勘探、资源评价、油气藏工程、油气田开发与开采、钻井和采油工程、油田化学、油气集输、石油机械等方面的论文。《石油学报》创刊于1980年，重点报道我国石油和天然气领域具有原创性的基础研究和应用研究成果，反映重大课题研究的最新进展，推广新技术和新方法，促进国内外石油科技学术交流。